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The chemistry of the Claus process involves partial oxidation of hydrogen sulfide to sulfur dioxide and the catalytically promoted reaction of hydrogen sulfide and sulfur dioxide to produce elemental sulfur The reactions are staged and are as follows: Thermal stage: H2S + 3/2 O2 SO2 + H2O Thermal and catalytic stage: SO2 + 2H2S 3S + 2H2O The efficiency of sulfur recovery depends upon such things as feed composition, age of the catalyst, and number of reactor stages Typical sulfur recovery efficiencies for Claus plants are 90 to 96 percent for a two-stage plant and 95 to 98 percent for a three-stage plant Because of equilibrium limitations and other sulfur losses, overall sulfur recovery efficiency in a Claus unit usually does not exceed 98 percent.

In 3, you learned how to specify the number of times an element and its children can be used in an XML document using a DTD. You can do something similar in an XML schema by using the minOccurs and maxOccurs attributes. The value of the minOccurs attribute determines the minimum number of times that an element must appear in the XML document. The value of the maxOccurs attribute determines the maximum number of occurrences for an element. You include the minOccurs and maxOccurs when you define the element, as shown here:

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The off-gas leaving a Claus plant is referred to as tail gas, and, in the past was burned to convert the unreacted hydrogen sulfide to sulfur dioxide, before discharge to the atmosphere, which has a much higher toxic limit However, the increasing standards of efficiency required by the pressure from environmental protection has led to the development of a large number of Claus tail gas clean-up units, based on different concepts, in order to remove the last remaining sulfur species (Gall and Gadelle, 2003) The oxygen-blown Claus process was originally developed to increase capacity at existing conventional Claus plants and to increase flame temperatures of gases having low hydrogen sulfide content The process has also been used to provide the capacity and operating flexibility for sulfur plants where the feed gas is variable in flow and composition such as often found in refineries.

Liquid redox sulfur recovery processes are liquid-phase oxidation processes which use a dilute aqueous solution of iron or vanadium to remove hydrogen sulfide selectively by chemical absorption from sour gas streams These processes can be used on relatively small or dilute hydrogen sulfide stream to recover sulfur from the acid gas stream or, in some cases, they can be used in place of an acid gas removal process The mildly alkaline lean liquid scrubs the hydrogen sulfide from the inlet gas stream, and the catalyst oxidizes the hydrogen sulfide to elemental sulfur The reduced catalyst is regenerated by contact with air in the oxidizer(s) Sulfur is removed from the solution by flotation or settling, depending on the process The wet oxidation processes are based on reduction-oxidation (redox) chemistry to oxidize the hydrogen sulfide to elemental sulfur in an alkaline solution containing an oxygen carrier.

In 15, Workflows and Transactions, we ll look at compensatable activities, including compensated transactions. Handling faults is part of the story. You can also compensate for them, which means to take action to mitigate the damage the exception might (or might not) cause.

Marketing newsletters have historically been printed items sent via snail mail Having a simple, physical newsletter to send to your customers has its benefits for eBay selling, too There s something special about getting mail especially if it s nicely designed and printed and full of useful information It sticks in the customer s mind better than an e-mail It causes them to pause and reflect on your business It lingers on their desktop and can be looked at repeatedly or passed on to a friend It reinforces your brand Plus, you don t have the worries of spam blockers preventing the delivery of your message or customers ignoring your e-mail and clicking the Delete button The benefit of e-mail newsletters is the interactivity they provide the customer.

Vanadium and iron are the two oxygen carriers that are used The best example of a process using the vanadium carrier is the Stretford process The most prominent examples of the processes using iron as a carrier are the LO-CAT process and the SulFerox process Both processes are capable of up to 99 percent or more sulfur recovery However, using the processes for Claus tail gas treating requires hydrolysis of all the sulfur dioxide in the tail gas to hydrogen sulfide because the sulfur dioxide will react with the buffering base potassium hydroxide (KOH) and form potassium sulfate (K2SO4) which will consume the buffering solution and quickly saturate it Tail gas-treating process involves the removal of the remaining sulfur compounds from gases remaining after sulfur recovery.

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